Structural Characterization of a Completely Alkyl-substituted Al-Sb Lewis Acid-base Adduct
In: Journal of Organometallic Chemistry, Jg. 695 (2010), S. 2281
Zeitschriftenaufsatz / Fach: Chemie
The Lewis acid–base adduct t-Bu3Al–SbMe3 (1), which was synthesized by reaction of equimolar amounts of t-Bu3Al and trimethylstibine SbMe3, was characterized by multinuclear NMR (1H, 13C) spectroscopy, elemental analyses as well as by single crystal X-ray diffraction.