Boese, Roland; Blaer, Dieter; Antipin, Mikhail Y.; Chaplinski, Vladmir; de Meijere, Armin:
Non-planar structures of Et3N and Pri3N: a contradiction between the X-ray, and NMR and electron diffraction data for Pri3N.
1998
In: Chemical Communications (Cambridge), Heft 7, S. 781 - 782
Artikel/Aufsatz in Zeitschrift1998Chemie
Titel:
Non-planar structures of Et3N and Pri3N: a contradiction between the X-ray, and NMR and electron diffraction data for Pri3N.
Autor(in):
Boese, RolandLSF; Blaer, Dieter; Antipin, Mikhail Y.; Chaplinski, Vladmir; de Meijere, Armin
Erscheinungsjahr
1998

Abstract:

The crystal structures of Et3N and Pri3N were detd. by x-ray anal. using the in situ crystn. technique for single crystal growth on the diffractometer; both have a pyramidal configuration of the N atom, even Pri3N, which was considered to be planar in accord with electron diffraction and NMR data. Crystallog. data are given.