Kuss, H.m.:

A new analyzer for quantitative sulfur determination.

In: CLB, Chemie fuer Labor und Betrieb, Jg. 39 (1988) ; Nr. 10, S. 494-495
ISSN: 0722-6764
Zeitschriftenaufsatz / Fach: Chemie
An analyzer is described for the detn. of S in org. and inorg. compds. The S-contg. compds. are reduced to H2S by HI, HCl, and NaH2PO2 at 135 Deg. The H2S gas is transferred into a H diffusion flame by an auxilliary gas (Ar or N). H2S forms S2 mols. in the flame. The chemiluminescence of this reaction is measured at 350-410 nm.