A solid-state NMR 3D heteronuclear dipolar-correlation experiment. The correlation of d(13C), d(15N), and D(C-N).
A 3D NMR expt. is proposed in which a 2D heteronuclear-correlation expt. is combined with the measurement of the heteronuclear dipolar coupling const. The pulse sequence is described. Tests were made on a 13C and 15N labeled glycine.
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