A new 2-dimensional(2D)-heteronuclear correlation pulse sequence for solids under magic-angle spinning conditions was developed. The expt. makes it possible to correlate spectra of 2 different nuclei through the weak heteronuclear dipolar coupling and provides an alternative when cross-polarization or the J-coupling are inappropriate for the transfer of coherence. This sequence was applied to aluminophosphate mol. sieve VPI-5.